| |
Organic compounds in soil, sludge and sediment
|
|
| |
|
| |
OJ-1 EPA-PAH | OJ-2 PCB | OJ-4 Phthalates | OJ-5 BTEX | OJ-6 Chlorinated aliphatics | OJ-7 Chlorophenols
OJ-8 Chlorobensener | OJ-11 Acetates | OJ-12 Screening | OJ-13 Screening | OJ-14 Solvents
OJ-17 Alkylbenzenes | OJ-18 Phenols | OJ-19 Organotin/organolead compounds, As speciation | OJ-20 Oil
OJ-21 SPIMFAB | OJ-22 Dioxins | OJ-23 Persistent organic compounds | OJ-24 Creosote
OJ-25 Brominated flame retardants | OJ-27 Nitrotoluenes | OJ-28 Pharmaceuticals | OJ-29 Terpenes
OJ-33 Aldehydes | PAH in asphalt | Oil identification | Other organic analyses
|
| |
|
| |
| OJ-1 Polycyclic aromatic hydrocarbons (EPA-PAH) in solid samples |
| naphthalene (0.1) |
benzo(b)fluoranthene (0.05) |
| acenaphthylene (0.1) |
benzo(k)fluoranthene (0.05) |
| acenaphthene (0.1) |
benzo(a)pyrene (0.05) |
| fluorene (0.1) |
dibenzo(ah) anthracene (0.05) |
| phenanthrene (0.1) |
benzo(ghi)perylene (0.05) |
| anthracene (0.1) |
indeno(123cd) pyrene (0.05) |
| fluoranthene (0.1) |
Sum of 16 EPA-PAHs (1.3) |
| pyrene (0.1) |
Sum of carcinogenic PAHs (0.2) |
| benzo(a)anthracene (0.05) |
Sum of non-carcinogenic PAHs (0.5) |
| chrysene (0.05) |
|
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: HPLC or GC-MS.
Analysis of PAHs by GC-MS is also available. Please contact the laboratory for more information.
PAHs in water, ash, biological samples and asphalt can also be determined. |
| |
|
| |
| OJ-1 sed Polycyclic aromatic hydrocarbons (EPA-PAH) in sediment |
| naphthalene (0.01) |
benzo(b)fluoranthene (0.01) |
| acenaphthylene (0.01) |
benzo(k)fluoranthene (0.01) |
| acenaphthene (0.01) |
benzo(a)pyrene (0.01) |
| fluorene (0.01) |
dibenzo(ah) anthracene (0.01) |
| phenanthrene (0.01) |
benzo(ghi)perylene (0.01) |
| anthracene (0.01) |
indeno(123cd) pyrene (0.01) |
| fluoranthene (0.01) |
Sum of 16 EPA-PAHs |
| pyrene (0.01) |
Sum of carcinogenic PAHs |
| benzo(a)anthracene (0.01) |
Sum of non-carcinogenic PAHs |
| chrysene (0.01) |
|
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 15 g dry matter in glass. Method: GC-MS.
|
| |
|
| |
| OJ-2a PCB in solid samples |
| PCB 28 |
PCB 138 |
| PCB 52 |
PCB 153 |
| PCB 101 |
PCB 180 |
| PCB 118 |
Sum of 7 PCBs |
|
|
Limit of quantification is 0.003 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-ECD or GC-MS.
Lower limits of quantification (0.1-0.3 µg/kg) can be achieved by using high-resolution GC-MS.
We can also determine PCB in water, fish, joint glue, oil and air. |
| |
|
| |
| OJ-2a sed PCB in sediment |
| PCB 28 |
PCB 138 |
| PCB 52 |
PCB 153 |
| PCB 101 |
PCB 180 |
| PCB 118 |
Sum of 7 PCBs |
|
|
Limit of quantification is 0.1 µg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 15 g dry matter in glass. Method: GC-MS. |
| |
|
| |
OJ-2b Coplanar and indicator PCBs
in solid samples |
| PCB 77 |
PCB 118 |
| PCB 105 |
PCB 167 |
| PCB 156 |
PCB 81 |
| PCB 126 |
PCB 123 |
| PCB 114 |
PCB 189 |
| PCB 157 |
Sum of PCBs WHO-TEQ |
| PCB 169 |
|
|
|
Limit of quantification is 0.1-0.3 µg/kg dry weight for each congener (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: HR-GC-MS.
ALS Scandinavia uses WHO factors to calculate toxic equivalents.
|
| |
|
| |
| OJ-4 Phthalates in solid samples |
| dimethylphthalate |
di-pentylphthalate |
| diethylphthalate |
di-n-octylphthalate (DNOP) |
| di-n-propylphthalate |
di-(2-ethylhexyl)phthalate (DEHP) |
| di-n-butylphthalate |
butylbenzylphthalate (BBP) |
| di-isobutylphthalate |
di-cyclohexylphthalate |
|
|
Limit of quantification is 0.8 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS or GC-ECD.
Supplementary analysis: didecylphthalate (DIDP) (10) + dinonylphthalate (DINP) (10)
|
| |
|
| |
OJ-5 Monoaromatic hydrocarbons (BTEX)
in solid samples |
| benzene |
ethylbenzene |
| toluene |
summa xylenes |
Limit of quantification is 0.02-0.2 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g drymatter in top-filled glass. Method: GC-MS. Price includes dry matter determination. |
|
|
| |
| OJ-5 + 1,2-dibromoethane + 1,2-dichloroethane |
| OJ-5 + monochlorobenzene |
Minimum sample amount: 50 g dry matter in top-filled glass. Method: GC-MS. |
|
| |
|
| |
| OJ-6 Chlorinated aliphatics in solid samples |
| dichloromethane |
trichloromethane |
| 1,1-dichloroethane |
tetrachloromethane |
| 1,2-dichloroethane |
1,1,1-trichloroethane |
| trans-1,2-dichloroethene |
1,1,2-trichloroethane |
| cis-1,2-dichloroethene |
trichloroethene |
| 1,2-dichloropropane |
tetrachloroethene |
|
|
Limit of quantification is 0.005-0.8 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Method: GC-MS or GC-ECD. OJ-6 may be supplemented with vinyl chloride.
Limit of quantification for vinyl chloride: 0.1 mg/kg. Minimum sample amount: 50 g dry matter in top-filled glass. Method: GC-MS. |
| |
|
| |
| OJ-7 Chlorophenols in solid samples |
| 2-monochlorophenol |
2,3,6-trichlorophenol |
| 3-monochlorophenol |
2,4,5-trichlorophenol |
| 4-monochlorophenol |
2,4,6-trichlorophenol |
| 2,3-dichlorophenol |
3,4,5-trichlorophenol |
| 2,4+2,5-dichlorophenol |
2,3,4,5-tetrachlorophenol |
| 2,6-dichlorophenol |
2,3,4,6-tetrachlorophenol |
| 3,4-dichlorophenol |
2,3,5,6-tetrachlorophenol |
| 3,5-dichlorophenol |
pentachlorophenol |
| 2,3,4-trichlorophenol |
Sum of chlorophenols |
| 2,3,5-trichlorophenol |
|
|
|
Limit of quantification is 0.02-0.1 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS.
|
| |
|
| |
| OJ-8 Chlorobenzenes in solid samples |
| monochlorobenzene |
| 1,2-dichlorobenzene |
| 1,3-dichlorobenzene |
| 1,4-dichlorobenzene |
| 1,2,3-trichlorobenzene |
| 1,2,4-trichlorobenzene |
| 1,3,5-trichlorobenzene |
| 1,2,3,4-tetrachlorobenzene |
| 1,2,3,5+1,2,4,5-tetrachlorobenzene |
| pentachlorobenzene |
| hexachlorobenzene |
| Sum of chlorobenzenes |
|
|
Limit of quantification is 0.01-0.05 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS or GC-ECD. |
| |
|
| |
| OJ-11 Acetates in solid samples |
| methylacetate |
iso-butylacetate |
| ethylacetate |
sec-butylacetate |
| n-propylacetate |
tert-butylacetate |
| iso-propylacetate |
n-pentylacetate |
| n-butylacetate |
iso-pentylacetate |
|
|
Limit of quantification is 0.5 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Method: GC-FID. |
| |
|
| |
| OJ-12a GC-MS screening for solid samples (semivolatile compounds) |
Aliphatics
aliphatics: >C10-C12 (20)
aliphatics: >C12-C16 (20)
aliphatics: >C16-C35 (20) |
| chlorobenzenes (1) |
| sum of PCBs (1) |
Polycyclic aromatic hydrocarbons
naphthalene (0.1)
acenaphthylene (0.1)
acenaphthene (0.1)
fluorene (0.1)
phenanthrene (0.1)
anthracene (0.1)
fluoranthene (0.1)
pyrene (0.1)
benso(a)anthracene (0.1)
chrysene (0.1)
benzo(b)fluoranthene (0.1)
benzo(k)fluoranthene (0.1)
benzo(a)pyrene (0.1)
dibenzo(ah)anthracene (0.1)
benzo(ghi)perylene (0.1)
indeno(123cd)pyrene (0.1)
Sum of 16 EPA-PAHs (1.3)
Sum of carcinogenic PAHs (0.2)
Sum of non-carcinogenic PAHs (0.5) |
| Other compounds |
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method (semi-quantitative): GC-MS.
OJ-12a may be combined with OJ-13a.
For "Other compounds" only compounds identified are reported (qualitative analysis). Semi-quantitative results can be obtained as a supplement. |
| |
|
| |
| OJ-13a GC-MS screening for solid samples (volatile compounds) |
Aliphatics
aliphatics>C5-C8 (10)
aliphatics>C8-C10 (10) |
Aromatics
benzene (0.05)
toluene (0.05)
etylbenzene (0.05)
sum of xylenes (0.05)
indane (0.05)
naphthalene (0.05)
sum of aromatics >C8-C10 (2) |
Chlorinated aliphatics
dichloromethane (0.1)
trichloromethane (chloroform) (0.1)
tetrachloromethane (0.1)
1,1-dichloroethane (0.1)
1,2-dichloroethane (0.1)
1,1,1-trichloroethane (0.1)
1,1,2-trichloroethane (0.1)
1,1,2,2-tetrachloroethane
1,2-dichloropropane (0.1)
cis-1,2-dichloroethene (0.1)
trans-1,2-dichloroethene (0.1)
trichloroethene (0.1)
tetrachloroethene (0.1) |
Chlorinated aromatics
monochlorobenzene (0.05)
dichlorobenzenes (0.1) |
| Other compounds |
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method (semi-quantitative): GC-MS.
This package can be ordered with vinyl chloride at no extra charge.
OJ-13a may be combined with OJ-12a.
For "Other compounds" only compounds identified are reported (qualitative analysis). Semi-quantitative results can be obtained as a supplement. |
| |
|
| |
OJ-14a Volatile organic compounds
in solid samples (VOC-EPA) |
Halogenated aliphatics
chloromethane (0.1)
bromomethane (0.1)
dichloromethane (0.8)
dibromomethane (0.1)
bromochloromethane (0.2)
trichloromethane (0.03)
tribromomethane (0.04)
bromodichloromethane (0.02)
dibromochloromethane (0.1)
tetrachloromethane (0.01)
trichlorofluormethane (0.1)
dichlorodifluormethane (0.1)
chloroethane (0.1)
1,1-dichloroethane (0.01)
1,2-dichloroethane (0.1)
1,2-dibromoethane (0.1)
1,1,1-trichloroethane (0.01)
1,1,2-trichloroethane (0.04)
1,1,1,2-tetrachloroethane (0.1)
1,1,2,2- tetrachloroethane (0.1)
vinyl chloride (0.1)
1,1-dichloroethene (0.01)
cis-1,2-dichloroethene (0.02)
trans-1,2-dichloroethene (0.01)
trichloroethene (0.01)
tetrachloroethene (0.02)
1,2-dichloropropane (0.1)
1,3-dichloropropane (0.1)
2,2-dichloropropane (0.1)
1,2,3-trichloropropane (0.1)
1,2-dibromo-3-chloropropane (0.1)
1,1-dichloro-1-propene (0.1)
cis-1,3-dichloro-1-propene (0.1)
trans-1,3-dichloro-1-propene (0.1)
hexachlorobutadiene (0.1) |
|
|
Halogenated aromatics
2-chlorotoluene (0.1)
4-chlorotoluene (0.1)
mono-chlorobenzene (0.1)
bromobenzene (0.1)
1,2-dichlorobenzene (0.02)
1,3-dichlorobenzene (0.02)
1,4-dichlorobenzene (0.02)
1,2,3- trichlorobenzene (0.02)
1,2,4- trichlorobenzene (0.03) |
Non-halogenated aromatics
benzene (0.02)
toluene (0.05)
ethylbenzene (0.1)
o-xylene (0.01)
m-xylene (0.02)
p-xylene (0.02)
styrene (0.02)
isopropylbenzene (0.1)
n-propylbenzene (0.1)
1,2,4- trimethylbenzene (0.1)
1,3,5- trimethylbenzene (0.1)
n-butylbenzene (0.1)
sec-butylbenzene (0.1)
tert-butylbenzene (0.1)
p-isopropyltoluene (0.1)
naphthalene (0.1) |
Figures in brackets denote limits of quantification in mg/kg dry weight. Minimum sample amount: 50 g dry matter in top-filled glass. Method: GC-MS. |
| |
|
| |
| OJ-17 Alkylbenzenes in solid samples |
| benzene |
n-propylbenzene |
| toluene |
1,3,5-trimethylbenzene |
| ethylbenzene |
tert-butylbenzene |
| m-xylene |
1,2,4-trimethylbenzene |
| p-xylene |
sec-butylbenzene |
| styrene |
p-isopropyltoluene |
| o-xylene |
n-butylbenzene |
| isopropylbenzene (kumene) |
|
|
|
Limit of quantification is 0.01-0.2 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Method: GC-MS. |
| |
|
| |
| OJ-18a Phenol, cresols and alkylphenols in solid samples |
| phenol |
|
| o-cresol |
|
| (m+p)-cresol |
|
| 2,3-dimethylphenol |
2,4,6-trimethylphenol |
| 2,4-dimethylphenol |
2-ethylphenol |
| 2,5-dimethylphenol |
3-ethylphenol |
| 2,6-dimethylphenol |
4-ethylphenol |
| 3,4-dimethylphenol |
2-n-propylphenol |
| 3,5-dimethylphenol |
2- isopropylphenol |
| 2,3,5-trimethylphenol |
3-tert-butylphenol |
|
|
Limit of quantification is 0.1 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. |
| |
|
| |
| OJ-18b Phenol and cresols in solid samples |
phenol
o-cesol
m-cresol
p-cresol |
| |
Limit of quantification is 0.1-1 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. |
| |
|
| |
OJ-18c Nonylphenol and octylphenol
in solid samples |
4-tert-octylphenol (0.01)
4-nonylphenol (0.1) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. |
| |
|
| |
OJ-18d Nonylphenol and -ethoxylates
in solid samples |
4-nonylphenol (10)
4-nonylphenol-monoethoxylate (10)
4-nonylphenol-diethoxylate (10) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. |
| |
|
| |
| OJ-18e Nonylphenol, octylphenol and ethoxylates in solid samples |
|
4-tert-octylphenol (0.01)
4-tert-octylphenol-monoethoxylate (0.01)
4-tert-octylphenol-diethoxylate (0.01)
4-tert-octylphenoltriethoxylate (0.01)
4-nonylphenol (0.1)
4-nonylphenol-monoethoxylate (0.1)
4-nonylphenol-diethoxylate (0.1)
4-nonylphenol-triethoxylate (0.1) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. |
| |
|
| |
OJ-19a Organotin compounds
in solid samples |
monobutyltin
dibutyltin
tributyltin (TBT)
tetrabutyltin
monooctyltin |
dioctyltin
tricyclohexyltin
monophenyltin
diphenyltin
triphenyltin |
|
|
Limit of quantification is 0.001 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-AED.
Determination of organotin compounds in water, fish, mussles, pine needles, tobacco etc is also available. |
| |
|
| |
| OJ-19b Organolead compounds in solid samples |
| tetramethyl lead |
| triethyl lead |
| diethyl lead |
| tetraethyl lead |
| |
Limit of quantification is 0.001 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-AED.
Determination of organolead compounds in water, fish, mussles, pine needles, tobacco etc is also available. |
| |
|
| |
OJ-19c Arsenic speciation for solid samples |
| As total |
Method: ICP-MS
Limit of quantification: 0.1 mg/kg |
arsenate
arsenite
monomethylarsonate
dimethylarsinate
trimethylarsinoxide
tetramethylarsonium ion
arsenobetaine
arsenocholine
arseno sugars |
Method: IC-ICP-MS.
Limit of quantification: 0.1-0.2 mg As/kg |
| |
Minimum sample amount: 50 g dry matter in glass.
|
| |
|
| |
| OJ-19d Arsenic speciation for solid samples |
As(III)
As(VI)
MMA(V) (monomethylarsonic)
DMA(V) (dimethylarsinic; cacodylate) |
|
|
Minimum sample amount: 5 g. |
| |
|
| |
| OJ-20a Oil analysis (Petrolpack) for solid samples |
benzene (0.05)
toluene (0.2)
ethylbenzene (0.05)
sum of xylenes (0.05)
aliphatics >C5-C8(10)
aliphatic >C8-C10(10)
fraction >C10-C12(20)
fraction >C12-C16(20)
fraction >C16-C35(50) |
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-FID/GC-MS. |
| |
|
| |
| OJ-20b Oil analysis (IR) for solid samples |
total extractable aliphatics
non-polar aliphatics
total extractable aromatics |
| |
Minimum sample amount: 50 g dry matter in glass. |
| |
|
| |
| OJ-20c Oil analysis (GC-FID) for solid samples |
| Mineral oil>C10-C40 (50) |
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. |
| |
|
| |
OJ-20d Oil analysis (MTBE) for solid samples |
| MTBE (0.2) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
OJ-20d may be combined with determination of TBA.
|
| |
|
| |
| OJ-20e Oil analysis (GC-FID) for solid samples |
fraction >C6-C16 (100)
fraction >C16-C35 (100) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight. Minimum sample amount: 50 g dry matter in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. |
| |
|
| |
| Oil identification for solid samples |
| comparison of chromatogram |
|
|
Reference sample included. Minimum sample amount: 100 g dry matter in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-FID. |
| |
|
| |
| OJ-21a Advanced GC-MS Package for soil (SPIMFAB) |
Aliphatics
aliphatics >C5-C8 (10)
aliphatics >C8-C10 (10)
aliphatics >C10-C12 (10)
aliphatics >C12-C16 (10)
aliphatics >C5-C16 (20)
aliphatics >C16-C35 (50) |
Aromatics
aromatics >C8-C10 (2)
aromatics >C10-C35 (2)
benzene (0.01)
toluene (0.05)
ethylbenzene (0.05)
sum of xylenes (0.05)
sum of TEX (0.08) |
Polycyclic aromatic hydrocarbons
naphthalene (0.1)
acenaphthylene (0.1)
acenaphthene (0.1)
fluorene (0.1)
phenanthrene (0.1)
anthracene (0.1)
fluoranthene (0.1)
pyrene (0.1)
benzo(a)anthracene (0.08)
chrysene (0.08)
benzo(b)fluoranthene (0.08)
benzo(k)fluoranthene (0.08)
benzo(a)pyrene (0.08)
dibenzo(ah)anthracene (0.08)
benzo(ghi)perylene (0.08)
indeno(123cd)pyrene (0.08)
Sum of 16 EPA-PAHs (1.3)
Sum of carcinogenic PAHs (0.3)
Sum of non-carcinogenic PAHs (0.5) |
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
|
| |
|
| |
| OJ-21b Advanced GC-MS Package for soil (SPIMFAB) |
Aliphatics
aliphatics >C5-C8 (10)
aliphatics >C8-C10 (10)
aliphatics >C10-C12 (10)
aliphatics >C12-C16 (10)
aliphatics >C5-C16 (20)
aliphatics >C16-C35 (50) |
Aromatics
aromatics >C8-C10 (2)
aromatics >C10-C35 (2)
benzene (0.01)
toluene (0.05)
ethylbenzene (0.05)
sum of xylenes (0.05)
sum of TEX (0.08) |
Polycyclic aromatic hydrocarbons
naphthalene (0.1)
acenaphthylene (0.1)
acenaphthene (0.1)
fluorene (0.1)
phenanthrene (0.1)
anthracene (0.1)
fluoranthene (0.1)
pyrene (0.1)
benzo(a)anthracene (0.08)
chrysene (0.08)
benzo(b)fluoranthene (0.08)
benzo(k)fluoranthene (0.08)
benzo(a)pyrene (0.08)
dibenzo(ah)anthracene (0.08)
benzo(ghi)perylene (0.08)
indeno(123cd)pyrene (0.08)
Sum of 16 EPA-PAHs (1.3)
Sum of carcinogenic PAHs (0.3)
Sum of non-carcinogenic PAHs (0.5) |
MTBE (metyl-tert-butyleter) (0.1)
1,2-dikloretan (0.1)
1,2-dibrometan (0.1) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
|
| |
|
| |
| OJ-21c Advanced GC-MS Package for soil (SPIMFAB) |
Aliphatics
aliphatics >C5-C8 (10)
aliphatics >C8-C10 (10)
aliphatics >C10-C12 (10)
aliphatics >C12-C16 (10)
aliphatics >C5-C16 (20)
aliphatics >C16-C35 (50) |
Aromatics
aromatics >C8-C10 (2)
aromatics >C10-C35 (2)
benzene (0.01)
toluene (0.05)
ethylbenzene (0.05)
sum of xylenes (0.05)
sum of TEX (0.08) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
|
| |
|
| |
| OJ-21d Advanced GC-MS Package for soil (SPIMFAB) |
Aliphatics
aliphatics >C10-C12 (10)
aliphatics >C12-C16 (10)
aliphatics >C16-C35 (50) |
Polycyclic aromatic hydrocarbons
naphthalene (0.1)
acenaphthylene (0.1)
acenaphthene (0.1)
fluorene (0.1)
phenanthrene (0.1)
anthracene (0.1)
fluoranthene (0.1)
pyrene (0.1)
benzo(a)anthracene (0.08)
chrysene (0.08)
benzo(b)fluoranthene (0.08)
benzo(k)fluoranthene (0.08)
benzo(a)pyrene (0.08)
dibenzo(ah)anthracene (0.08)
benzo(ghi)perylene (0.08)
indeno(123cd)pyrene (0.08)
Sum of 16 EPA-PAHs (1.3)
Sum of carcinogenic PAHs (0.3)
Sum of non-carcinogenic PAHs (0.5) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
|
| |
|
| |
| OJ-21e Advanced GC-MS Package for soil (SPIMFAB) |
Aliphatics
aliphatics >C5-C8 (10)
aliphatics >C8-C10 (10)
aliphatics >C10-C12 (10)
aliphatics >C12-C16 (10)
aliphatics >C5-C16 (20)
aliphatics >C16-C35 (50) |
Polycyclic aromatic hydrocarbons
naphthalene (0.1)
acenaphthylene (0.1)
acenaphthene (0.1)
fluorene (0.1)
phenanthrene (0.1)
anthracene (0.1)
fluoranthene (0.1)
pyrene (0.1)
benzo(a)anthracene (0.08)
chrysene (0.08)
benzo(b)fluoranthene (0.08)
benzo(k)fluoranthene (0.08)
benzo(a)pyrene (0.08)
dibenzo(ah)anthracene (0.08)
benzo(ghi)perylene (0.08)
indeno(123cd)pyrene (0.08)
Sum of 16 EPA-PAHs (1.3)
Sum of carcinogenic PAHs (0.3)
Sum of non-carcinogenic PAHs (0.5) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS according to SPIMFAB/SNV 4889.
|
| |
|
| |
| OJ-21f Advanced GC-MS Package for soil (SPIMFAB) |
Aliphatics
aliphatics >C5-C8 (10)
aliphatics >C8-C10 (10)
aliphatics >C10-C12 (10)
aliphatics >C12-C16 (10)
aliphatics >C5-C16 (20)
aliphatics >C16-C35 (50) |
Aromatics
aromatics >C8-C10 (2)
aromatics >C10-C35 (2) |
Polycyclic aromatic hydrocarbons
naphthalene (0.1)
acenaphthylene (0.1)
acenaphthene (0.1)
fluorene (0.1)
phenanthrene (0.1)
anthracene (0.1)
fluoranthene (0.1)
pyrene (0.1)
benzo(a)anthracene (0.08)
chrysene (0.08)
benzo(b)fluoranthene (0.08)
benzo(k)fluoranthene (0.08)
benzo(a)pyrene (0.08)
dibenzo(ah)anthracene (0.08)
benzo(ghi)perylene (0.08)
indeno(123cd)pyrene (0.08)
Sum of 16 EPA-PAHs (1.3)
Sum of carcinogenic PAHs (0.3)
Sum of non-carcinogenic PAHs (0.5) |
| |
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
|
| |
|
| |
| OJ-21h Advanced GC-MS Package for soil (SPIMFAB) |
Aliphatics
aliphatics >C8-C10 (10)
aliphatics >C10-C12 (10)
aliphatics >C12-C16 (10)
aliphatics >C16-C35 (50) |
Aromatics
aromatics >C8-C10 (2)
aromatics >C10-C35 (2) |
Polycyclic aromatic hydrocarbons
naphthalene (0.1)
acenaphthylene (0.1)
acenaphthene (0.1)
fluorene (0.1)
phenanthrene (0.1)
anthracene (0.1)
fluoranthene (0.1)
pyrene (0.1)
benzo(a)anthracene (0.08)
chrysene (0.08)
benzo(b)fluoranthene (0.08)
benzo(k)fluoranthene (0.08)
benzo(a)pyrene (0.08)
dibenzo(ah)anthracene (0.08)
benzo(ghi)perylene (0.08)
indeno(123cd)pyrene (0.08)
Sum of 16 EPA-PAHs (1.3)
Sum of carcinogenic PAHs (0.3)
Sum of non-carcinogenic PAHs (0.5) |
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
|
| |
|
| |
| OJ-22 Dioxins and furans in solid samples |
2,3,7,8-tetraCDD (1)
1,2,3,7,8-pentaCDD(2)
1,2,3,4,7,8-hexaCDD (3)
1,2,3,6,7,8-hexaCDD (3)
1,2,3,7,8,9-hexaCDD (3)
1,2,3,4,6,7,8-heptaCDD (5)
octachlorodibenzodioxin (10)
2,3,7,8-tetraCDF (1)
1,2,3,7,8-pentaCDF (2)
2,3,4,7,8-pentaCDF (2)
1,2,3,4,7,8-hexaCDF (3)
1,2,3,6,7,8-hexaCDF (3)
1,2,3,7,8,9-hexaCDF (3)
2,3,4,6,7,8-hexaCDF (3)
1,2,3,4,6,7,8-heptaCDF (5)
1,2,3,4,7,8,9-heptaCDF (5)
octachlorodibenzofuran (10)
sum of PCDD/PCDF WHO-TEQ |
|
|
Figures in brackets denote limits of quantification in ng/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: HR-GC-MS.
Supplementary analysis:
OJ-2b Dioxin-like PCBs in solid samples |
PCB 77
PCB 126
PCB 169
PCB 81 |
PCB 105
PCB 114
PCB 118
PCB 123 |
PCB 156
PCB 157
PCB 167
PCB 189 |
Limit of quantification is 0.1-0.3 µg/kg dry weight for each congener.
|
| |
|
| |
| OJ-23 Persistant organic compounds in sludge * |
Polycyclic aromatic hydrocarbons
naphthalene (0.05)
acenaphthylene (0.05)
acenaphthene (0.05)
fluorene (0.05)
phenanthrene (0.05)
anthracene (0.05)
fluoranthene (0.05)
pyrene (0.05)
benzo(a)anthracene (0.05)
chrysene (0.05)
benzo(b)fluoranthene (0.05)
benzo(k)fluoranthene (0.05)
benzo(a)pyrene (0.05)
dibenzo(ah)anthracene (0.05)
benzo(ghi)perylene (0.05)
indeno(123cd)pyrene (0.05)
Sum of 16 EPA-PAHs (0.4)
Sum of carcinogenic PAHs (0.2)
Sum of non-carcinogenic PAHs (0.2) |
| Polychlorinated biphenyls (PCB) |
PCB 28 (0.003)
PCB 52 (0.003)
PCB 101 (0.003)
PCB 118 (0.003) |
PCB 138 (0.003)
PCB 153 (0.003)
PCB 180 (0.003)
Sum of 7 PCBs (0.01) |
toluene (0.03)
4-nonylphenol (0.1) |
* According to Report 3829, Swedish EPA (Naturvårdsverket) |
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. Price includes dry matter determination.
|
| |
|
| |
| OJ-24a Creosotes in solid samples |
naphthalene
acenaphthylene
acenaphthene
fluorene
phenanthrene
anthracene
fluoranthene
pyrene
benzo(a)anthracene
chrysene
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
dibenzo(ah)anthracene
benzo(ghi)perylene
indeno(123cd)pyrene
Sum of 16 EPA-PAHs
Sum of carcinogenic PAHs
Sum of non-carcinogenic PAHs
benzo(e)pyrene
1-methylnaftalene
2-methylnaftalene
biphenyl |
|
|
Limit of quantification is 0.05 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g in glass. Method: GC-MS. |
| |
|
| |
| OJ-24b Creosotes in solid sampless |
PAHs
naphthalene
acenaphthylene
acenaphthene
fluorene
phenanthrene
anthracene
fluoranthene
pyrene
benzo(a)anthracene
chrysene
benzo(b)fluoranthene
benzo(k)fluoranthene
benzo(a)pyrene
dibenzo(ah)anthracene
benzo(ghi)perylene
indeno(123cd)pyrene
Sum of 16 EPA-PAHs
Sum of carcinogenic PAHs
Sum of non-carcinogenic PAHs
benzo(e)pyrene
1-methylnaphthalene
2-methylnaphthalene
biphenyl |
Phenols
o-cresol
m-cresol
p-cresol |
O-heterocycles
dibenzofuran |
N-heterocycles
quinoline
iso-quinoline
carbazole |
S-heterocycles
dibenzothiophene |
| |
Limit of quantification is 0.05-0.1 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g in glass. Method: GC-MS. |
| |
|
| |
| OJ-25 Brominated flame retardants in solid samples |
tetraBDE (0.5)
pentaBDE (0.5)
PBDE 47 (0.05)
PBDE 99 (0.05)
hexaBDE (0.5)
PBDE 100 (0.05)
heptaBDE (1)
octaBDE (1)
nonaBDE (1)
decaBDE (5)
tetrabromobisphenol-A (TBBP-A) (0.5)
decabromobiphenyl (DeBB) (5)
hexabromocyclododecane (HBCD) (5) |
|
|
Figures in brackets denote limits of quantification in µg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. |
| |
|
| |
| OJ-27a Nitrotoluenes in solid samples |
2,4,6-trinitrotoluene (TNT)
2,3-dinitrotoluene
2,4-dinitrotoluene
2,6-dinitrotoluene
3,4-dinitrotoluene
2-nitrotoluene
3-nitrotoluene
4-nitrotoluene |
|
|
Limit of quantification is 0.05 mg/kg. Minimum sample amount: 50 g dry matter in glass. Method: GC-MS. |
| |
|
| |
| OJ-27b RDX + HMX + TNT in solid samples |
| RDX (hexogen) (0.1)
HMX (octogen) (0.1)
TNT (trotyl) (0.1)
|
|
|
Figures in brackets denote limits of quantification in mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in glass. Method: HPLC-DAD. |
| |
|
| |
| OJ-28c Pharmaceuticals in solid samples |
atenolol
citalopram
cyclophosphamide
diazepam
diclofenac
doxycycline
enalapril
estradiol
estriol
ethynylestradiol
fluoxetine
furosemide
hydrochlorhthiazide
ipuprofen
ifosmamide
ketoprofen
metformin
metoprolol
naproxen
norethisterone
oxazepam
oxitetracycline
paracetamol
ranitidine
salbutamol
sertraline
simvastatin
terbutaline
tetracycline
warfarin
|
|
|
Limit of quantification is 0.01-0.1 mg/kg dry weight . Minimum sample amount: 50 g dry matter in glass. Method: LC-MS-MS, GC-MS. |
| |
|
| |
| OJ-29 Terpenes in solid samples |
a-pinene
ß-pinene
3-carene
limonene |
|
|
Limit of quantification is 0.05 mg/kg (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: GC-MS.
OJ-29 may be supplemented with the analysis of camphene and camphor. |
| |
|
| |
| OJ-32 Chloroparaffins in solid samples |
C10-C13 (SCCP)
C14-C17 (MCCP) |
|
|
Limit of quantification is 0.010 mg/kg dry weight (may vary depending on sample composition). Minimum sample amount: 50 g dry matter. Method: GC-MS. |
| |
|
| |
| OJ-33 Aldehydes in solid samples |
formaldehyde (methanal)
acetaldehyde (ethanal)
propional
butanal
glutaraldehyde (pentadial) |
|
|
Limit of quantification is 0.010 mg/kg (may vary depending on sample composition). Minimum sample amount: 50 g dry matter in top-filled glass. Note: The sample must be sent cooled to the laboratory without delay. Method: HPLC-DAD. |
| |
|
| |
| PAH in asphalt |
| naphthalene (0.1) |
benzo(b)fluoranthene (0.05) |
| acenaphthylene (0.1) |
benzo(k)fluoranthene (0.05) |
| acenaphthene (0.1) |
benzo(a)pyrene (0.05) |
| fluorene (0.1) |
dibenzo(ah) anthracene (0.05) |
| phenanthrene (0.1) |
benzo(ghi)perylene (0.05) |
| anthracene (0.1) |
indeno(123cd) pyrene (0.05) |
| fluoranthene (0.1) |
Sum of 16 EPA-PAHs (1.3) |
| pyrene (0.1) |
Sum of carcinogenic PAHs (0.2) |
| benzo(a)anthracen (0.05) |
Sum of non-carcinogenic PAHs (0.5) |
| chrysene (0.05) |
|
|
|
Minimum sample amount: 50 g dry matter. Sample preparation not included. Method: GC-MS/HP-LC. |
| |
|
| |
| Other organic analyses |
| EGOM |
| AOX |
| EOX |
| epichlorohydrin |
| phenol index |
| formaldehyde (spectrophotometry) |
| formaldehyde (HPLC) |
| glycols (ethylen glycol, propylen glycol |
| MTBE |
|
|
|
| |
|
| |
| Sample preparation |
| |
| Solid samples: |
| Cryogenic grinding |
| Grinding in rotary cutter |
| Grinding in steel drum |
| DMSO cleanup |
| Removal of humic compounds |
|
|
|
| |
|
| |
Determination of other compounds is available. Please contact the laboratory for information.
|
|
|
|